HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylamine → HCID 178484394, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | 1,1-Bis(methylthio)-2-nitroethylene | HCID 83623 | — |
| Reactant | 1-Nitro-2-methylthio-2-[4-(4-imidazolyl)butylamino]ethylene | HCID 178503821 | — |
| Reactant | HCID 178510959 | HCID 178510959 | — |
| Product | HCID 178484394 | HCID 178484394 | — |
Reaction Steps
Reaction of 4-(4-aminobutyl)imidazole (from the dihydrobromide (3.6 g)) with 1-nitro-2,2-bis-methylthioethylene (2.0 g) by the procedure of Example 4(i) and treatment of the resultant 1-nitro-2-methylthio-2-[4-(4-imidazolyl)butylamino]ethylene with methylamine according to the procedure of Example 3(ii) gives the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04024260 |
| Source dataset | uspto-grants-1977_05 |
| ORD ID | ord-b296e926ea0c4be6a1f23703e9370df3 |
| Source note | uspto-grants-1977_05 |