HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanone, (4-methoxyphenyl)(2-phenyl-3-benzofuranyl)- → (4-Hydroxyphenyl)(2-phenyl-1-benzofuran-3-yl)methanone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanone, (4-methoxyphenyl)(2-phenyl-3-benzofuranyl)- | HCID 6613416 | — |
| Reactant | Pyridinium chloride | HCID 10176127 | — |
| Product | (4-Hydroxyphenyl)(2-phenyl-1-benzofuran-3-yl)methanone | HCID 13264991 | — |
Reaction Steps
3-(4-Methoxybenzoyl)-2-phenylbenzofuran (16.4 g., 0.05 mol.) is combined with 50 g. of freshly distilled pyridine hydrochloride and the mixture is refluxed one hour. The hot mixture is poured with stirring onto an ice-dilute hydrochloric acid mixture and the precipitate is collected to give 3-(4-hydroxybenzoyl)-2-phenylbenzofuran.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04024273 |
| Source dataset | uspto-grants-1977_05 |
| ORD ID | ord-73a56a9b62f84a449736bfa1d50dd343 |
| Source note | uspto-grants-1977_05 |