HRID2398447

反应详情

EQUATION

反应方程式

HRID 2398447 的结构方程式

PROCEDURE

实验过程

3-(3,5-Dimethyl-4-methoxybenzoyl)-2-phenylbenzofuran (17.8 g., 0.05 mol.) is combined with 50 g. of freshly distilled pyridine hydrochloride and the mixture is refluxed one hour. The hot mixture is poured with stirring onto an ice-dilute hydrochloric acid mixture and the precipitate is collected to give 3-(3,5-dimethyl-4-hydroxybenzoyl)-2-phenylbenzofuran.

WORKUP

后处理

  1. additionThe hot mixture is poured
  2. customthe precipitate is collected