HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridinium chloride → 3-(3,5-Dimethyl-4-hydroxybenzoyl)-2-phenylbenzofuran
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridinium chloride | HCID 10176127 | — |
| Reactant | 3-(3,5-Dimethyl-4-methoxybenzoyl)-2-phenylbenzofuran | HCID 21435358 | — |
| Product | 3-(3,5-Dimethyl-4-hydroxybenzoyl)-2-phenylbenzofuran | HCID 21435273 | — |
Reaction Steps
3-(3,5-Dimethyl-4-methoxybenzoyl)-2-phenylbenzofuran (17.8 g., 0.05 mol.) is combined with 50 g. of freshly distilled pyridine hydrochloride and the mixture is refluxed one hour. The hot mixture is poured with stirring onto an ice-dilute hydrochloric acid mixture and the precipitate is collected to give 3-(3,5-dimethyl-4-hydroxybenzoyl)-2-phenylbenzofuran.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04024273 |
| Source dataset | uspto-grants-1977_05 |
| ORD ID | ord-e0d9d3ff8c97425e9087045439e75f9b |
| Source note | uspto-grants-1977_05 |