HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Nitro-2-nitrosocyclooctane → N-(2-Nitrocyclooctylidene)hydroxylamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Nitro-2-nitrosocyclooctane | HCID 21435616 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | N-(2-Nitrocyclooctylidene)hydroxylamine | HCID 71358152 | — |
Reaction Steps
1-Nitroso-2-nitrocyclooctane, in a three-fold amount of dioxane, is heated for 2 hours under nitrogen at 100° C, whilst stirring. After removing the solvent on a rotary evaporator, 2-nitro-cyclooctan-1-one-oxime is obtained, in quantitative yield, as a brown oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04024327 |
| Source dataset | uspto-grants-1977_05 |
| ORD ID | ord-64b4f84d4e2949748987e99f2e383982 |
| Source note | uspto-grants-1977_05 |