HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 68118800, compound → HCID 68119677, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 68118800 | HCID 68118800 | — |
| Catalyst | Platinum oxide (PtO) | HCID 82844 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 68119677 | HCID 68119677 | — |
Reaction Steps
The mixture of 1.5 g of N-(4-nitro-o-tolyl)-4-carbamoylphthalimide 200 ml of ethyl acetate and 0.3 g of platinum oxide is hydrogenated at 2.5 atm. and about 40° for 50 minutes. It is filtered, the filtrate concentrated and the precipitate collected, to yield the N-(4-amino-o-tolyl)-4-carbamoylphthalimide melting at 240°-242°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04025505 |
| Source dataset | uspto-grants-1977_05 |
| ORD ID | ord-9a2d36da408648bfb0140edc3085b26e |
| Source note | uspto-grants-1977_05 |