HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → HCID 68118813, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | 4-Chlorophthalic anhydride | HCID 67044 | — |
| Reactant | 4-Amino-3-methylbenzoic acid | HCID 75598 | — |
| Product | HCID 68118813 | HCID 68118813 | — |
Reaction Steps
The starting material is prepared as follows: The suspension of 6.0 g of 4-chlorophthalic anhydride, 5.0 g of 4-amino-3-methylbenzoic acid and 75 ml of acetic acid is refluxed for 3 hours, cooled to room temperature, filtered and the residue washed with diethyl ethyl, to yield the N-(4-carboxy-o-tolyl)-4-chlorophthalimide melting at 250°-252°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04025505 |
| Source dataset | uspto-grants-1977_05 |
| ORD ID | ord-833f211144aa4967b44c6dd860757b69 |
| Source note | uspto-grants-1977_05 |