Hydrochloric Acid → HCID 12653318, compound

HRID 2398611Notes

Reaction equation

HRID 2398611 reaction equation
[CH3:1][C:2]([CH3:6])([OH:5])[C:3]#[N:4].[CH2:7]([O:9]CC)[CH3:8].[ClH:12]>C(O)C>[ClH:12].[CH3:1][C:2]([CH3:6])([OH:5])[C:3](=[NH:4])[O:9][CH2:7][CH3:8]

Participants

5

Reactant 3

HCID 313Hydrochloric AcidHCID 3283Diethyl EtherHCID 6406Acetone Cyanohydrin

Product 1

HCID 12653318HCID 12653318, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

Four grams of 2-methyllactonitrile is added to 100 ml. of diethyl ether containing 10 ml. of ethanol followed by saturation of the resulting solution with hydrogen chloride gas. The reaction mixture is allowed to stir at room temperature for 18 hrs. and subsequently concentrated to an oil which on slurrying in ether gave 7.2 g. of the desired product.

Workup

  1. concentrationand subsequently concentrated to an oil which on slurrying in ether
  2. customgave 7.2 g

Sources & evidence

ORD record
ord-3b93632eedb945c0b4e154a4e459513b
Source dataset
uspto-grants-1977_05
Patent number
US04025504

Reaction notes

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