HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 12452841, compound → 2-Methyl-5-(propan-2-yl)furan-3-carboxylic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 12452841 | HCID 12452841 | — |
| Solvent | Sodium Hydroxide | HCID 14798 | — |
| Product | 2-Methyl-5-(propan-2-yl)furan-3-carboxylic acid | HCID 21433405 | — |
Reaction Steps
Saponification of 0.5 g of the ester was accomplished by refluxing 4 hours in 10 ml of 25% aqueous sodium hydroxide. Acidification precipitated the crude acid, which was recrystallized from water-ethanol to give 5isopropyl-2-methyl-3-furoic acid as white needles, mp 88.5° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04025537 |
| Source dataset | uspto-grants-1977_05 |
| ORD ID | ord-b1a5232e58be4758b755d18eaec55a79 |
| Source note | uspto-grants-1977_05 |