HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 12452845, compound → HCID 21433408, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 12452845 | HCID 12452845 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Sodium Hydroxide | HCID 14798 | — |
| Product | HCID 21433408 | HCID 21433408 | — |
Reaction Steps
Saponification of 0.5 g of the ester was carried out by refluxing 12 hours in 10 ml of 25% aqueous sodium hydroxide and 5 ml of ethanol. Acidification precipitated the crude acid which was purified by sublimination to give 5-methyl-2-propyl-3-furoic acid, mp 91°-102° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04025537 |
| Source dataset | uspto-grants-1977_05 |
| ORD ID | ord-a613d4d8ab324bd7859b0b067c6edd91 |
| Source note | uspto-grants-1977_05 |