HuagongsheHuagongshe Chemistry Print Report · For research reference only
Octane → HCID 12783668, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Octane | HCID 356 | — |
| Reactant | Dichloromethane | HCID 6344 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | Tetramethylphosphanium iodide | HCID 120511 | — |
| Reactant | HCID 138767 | HCID 138767 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 12783668 | HCID 12783668 | — |
Reaction Steps
Cyclotetradecene (4.0 g), chloroform (18 ml), 50% aqueous sodium hydroxide solution (22 ml), dichloromethane (5 ml), n-octane (1 ml) and tetramethylphosphonium iodide (0.01 g) were stirred together at 35° C. for 3 hours. At the end of this period the conversion of starting material to the desired product was found by GLC to be 100%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04025562 |
| Source dataset | uspto-grants-1977_05 |
| ORD ID | ord-5f5ee7364deb44bd82132d9659134717 |
| Source note | uspto-grants-1977_05 |