Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2398709Generated: October 31, 2026

Octane → HCID 12323991, compound

https://huagongshe.com/reaction/2398709

Reaction equation

Participants

RoleNameHCIDCharge
ReactantOctaneHCID 356—
Reactant1,1-DichloroethaneHCID 6365—
ReactantSodium HydroxideHCID 14798—
ReactantCyclododecene, (E)-HCID 15164—
ReactantHCID 20289373HCID 20289373—
SolventChloroformHCID 6212—
ProductHCID 12323991HCID 1232399198%

Reaction Steps

Cyclododecene (41.5 g), chloroform (225 ml), 50% aqueous sodium hydroxide solution (275 ml), dichloroethane (60 ml), sec-hexadecyl sec-dodecyl ethylsulphonium ethylsulphate (0.3 g) and n-octane (12 ml) were stirred together at ambient temperature for 10 hours. The product was recovered in a similar manner to that described in Example I(b) (yield 98%)

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04025562
Source datasetuspto-grants-1977_05
ORD IDord-507f8e9bbab3494e887b689a82439e56
Source noteuspto-grants-1977_05