HuagongsheHuagongshe Chemistry Print Report · For research reference only
Octane → HCID 12323991, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Octane | HCID 356 | — |
| Reactant | 1,1-Dichloroethane | HCID 6365 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | Cyclododecene, (E)- | HCID 15164 | — |
| Reactant | HCID 20289373 | HCID 20289373 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 12323991 | HCID 12323991 | 98% |
Reaction Steps
Cyclododecene (41.5 g), chloroform (225 ml), 50% aqueous sodium hydroxide solution (275 ml), dichloroethane (60 ml), sec-hexadecyl sec-dodecyl ethylsulphonium ethylsulphate (0.3 g) and n-octane (12 ml) were stirred together at ambient temperature for 10 hours. The product was recovered in a similar manner to that described in Example I(b) (yield 98%)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04025562 |
| Source dataset | uspto-grants-1977_05 |
| ORD ID | ord-507f8e9bbab3494e887b689a82439e56 |
| Source note | uspto-grants-1977_05 |