HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 66680818, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 11219755 | HCID 11219755 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 66680818 | HCID 66680818 | 81.2% |
Reaction Steps
A solution of Example 53A (140 mg) in 1:1 methanol/10% NaOH (1 mL) was stirred at room temperature for 2 hours and adjusted to pH 3 with 10% HCl. The resulting precipitate was collected by filtration to provide 108 mg of the desired product. MS (ESI(+)) m/e 268 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08642776B2 |
| Source dataset | uspto-grants-2014_02 |
| ORD ID | ord-0187ebcc30c94d7da35c30b236720340 |
| Source note | uspto-grants-2014_02 |