HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl N-cyanocarbamate → 5-Cyclohexylethylthio-2-carbomethoxyaminobenzimidazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl N-cyanocarbamate | HCID 89023 | — |
| Reactant | 2-Nitro-5-cyclohexylethylthioaniline | HCID 54479877 | — |
| Product | 5-Cyclohexylethylthio-2-carbomethoxyaminobenzimidazole | HCID 54415697 | — |
Reaction Steps
Repeating the reaction of Example 1 but using 10.0 g. of cyclohexylethylthiol gives 2-nitro-5-cyclohexylethylthioaniline. The nitro compound is reduced. The reduction mixture is reacted with carbomethoxycyanamide as described to give 5-cyclohexylethylthio-2-carbomethoxyaminobenzimidazole.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04025638 |
| Source dataset | uspto-grants-1977_05 |
| ORD ID | ord-daa640345104442a88f6a1a9fd58de27 |
| Source note | uspto-grants-1977_05 |