HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Thiophenecarboxylic acid, tetrahydro-3-oxo-, methyl ester → 7-(3-cyclopropyl-2-propyl)-1,2-dihydro9-hydroxy-4-oxo-4H-thieno[2,3-c][1]benzopyran
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Thiophenecarboxylic acid, tetrahydro-3-oxo-, methyl ester | HCID 102870 | — |
| Reactant | 5-(3-Cyclopropyl-2-propyl)resorcinol | HCID 53843496 | — |
| Product | 7-(3-cyclopropyl-2-propyl)-1,2-dihydro9-hydroxy-4-oxo-4H-thieno[2,3-c][1]benzopyran | HCID 21433870 | — |
Reaction Steps
Following a procedure similar to that described in Example 1B hereinabove, methyl 3-oxo-2,3,4,5-tetrahydrothiophene-2-carboxylate is reacted with 5-(3-cyclopropyl-2-propyl)resorcinol to give 7-(3-cyclopropyl-2-propyl)-1,2-dihydro-9-hydroxy-4-oxo-4H-thieno[2,3-c][1]benzopyran.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04025630 |
| Source dataset | uspto-grants-1977_05 |
| ORD ID | ord-a934d346eeb74814bf8aca10ecb3c493 |
| Source note | uspto-grants-1977_05 |