HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine hydrate (1:1) → HCID 21432164, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Reactant | HCID 21432172 | HCID 21432172 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 21432164 | HCID 21432164 | — |
Reaction Steps
32.5 gm of 3-(3'-nitro-4'-acetylamino-benzoyl)-propionic acid were added toa solution of 32.5 gm of hydrazine hydrate in 180 ml of glacial acetic acid, and the mixture was heated on a steam bath. After cooling, the precipitate formed thereby was suction-filtered off and washed with ether,yielding the desired compound; m.p. 223° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04026891 |
| Source dataset | uspto-grants-1977_05 |
| ORD ID | ord-244fd778e2cb4baa9c27f04b9e53b9e4 |
| Source note | uspto-grants-1977_05 |