HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trimethyl Phosphate → 1,2,3,8-Tetrahydro-1,2,3,3,8-pentamethyl-5-(trifluoromethyl)-7H-pyrrolo(3,2-g)quinolin-7-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trimethyl Phosphate | HCID 10541 | — |
| Reactant | 7-oxo-1,2,3,3-tetramethyl-5-trifluoromethyl-2,3,7,8-tetrahydro-1H-pyrrolo [3,2-g] quinoline | HCID 323233 | — |
| Product | 1,2,3,8-Tetrahydro-1,2,3,3,8-pentamethyl-5-(trifluoromethyl)-7H-pyrrolo(3,2-g)quinolin-7-one | HCID 93886 | — |
Reaction Steps
refluxing said 7-oxo-1,2,3,3-tetramethyl-5-trifluoromethyl-2,3,7,8-tetrahydro-1H-pyrrolo [3,2-g] quinoline with trimethyl phosphate to yield 7-oxo-1,2,3,3,8-pentamethyl-5-trifluoromethyl-2,3,7,8-tetrahydro-1H-pyrrolo [3,2-g] quinoline.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04026898 |
| Source dataset | uspto-grants-1977_05 |
| ORD ID | ord-110aafcee05244178bc4f32f62c00024 |
| Source note | uspto-grants-1977_05 |