Nitrobenzene → HCID 178481318, compound

Participants

Reaction Steps

In 110 ml. of nitrobenzene, 7.6 g. (0.029 mole) of 2-(1-methyl-5-nitro-2-imidazolecarboximidoyl)-1-amidinohydrazine hydrocloride is stirred at reflux temperature for 23/4 hours, cooled, and the solid collected. This solid is washed with ethyl alcohol, ether, and air-dried to give 6 g. of the title compound, melting point 278°-280° (dec.). The product is purified by removing soluble impurities in a Soxhlet extractor with 95% ethanol. The insoluble products melts at 297°-299° (dec.).

Provenance & Evidence