HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thiosemicarbazide → HCID 178481319, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thiosemicarbazide | HCID 2723789 | — |
| Reactant | Ethyl 1-methyl-5-nitro-1H-imidazole-2-carboximidate | HCID 21432269 | — |
| Catalyst | Sulfuric Acid | HCID 1118 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 178481319 | HCID 178481319 | — |
Reaction Steps
To a stirred mixture of ethyl 1-methyl-5-nitro-2-imidazolecarboximidate (0.198 g., 0.001 mole) and thiosemicarbazide (0.091 g., 0.001 mole) in 5 ml. of methanol is added 1 drop of conc. H2SO4 and the mixture is stirred at room temperature for 50 minutes. The solid is filtered and washed with methanol, yielding 0.149 g. of the title compound, melting point 200°-201° C. dec.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04026903 |
| Source dataset | uspto-grants-1977_05 |
| ORD ID | ord-f8c6d7817d5a4d9a905674142f54b989 |
| Source note | uspto-grants-1977_05 |