4-Aminophenylacetic acid → HCID 70560746, compound

Participants

Reaction Steps

p-Aminophenylacetic acid (3.02 g) was dissolved in 51.9 g of 10% aqueous tetrabutylammonium hydroxide, and the solution was evaporated under reduced pressure to an amber oil. Upon further drying at 0.1 mm pressure at room temperature, a green solid was obtained. After rinsing with tetrahydrofuran there was obtained 4.696 g of nearly colorless crystals of tetrabutylammonium p-aminophenylacetate.

Provenance & Evidence