Ammonia → HCID 21432748, compound

Participants

Reaction Steps

Aqueous ammonia solution (specific gravity 0.88; 10 ml.) was added to 6-ethylcinnolin-3-yl carbonyl chloride (1 g.). The resulting suspension was stirred overnight at room temperature. The resulting mixture was filtered and the solid residue was crystallised from aqueous ethanol to give 6-ethylcinnolin-3-ylcarboxamide, m.p. 215°-216° C.

Provenance & Evidence