HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen Bromide → HCID 86734797, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen Bromide | HCID 260 | — |
| Reactant | 3-Amino-1-propanol | HCID 9086 | — |
| Reactant | HCID 178418616 | HCID 178418616 | — |
| Product | HCID 86734797 | HCID 86734797 | — |
Reaction Steps
A solution of 2-mercaptopyridine (2.2 g.) and 3-aminopropanol (1.14 ml.) in hydrobromic acid (48%, 25 ml.) was heated under reflux for 25 hours. The reaction mixture was evaporated to dryness and the oily residual solid recrystallised twice from ethanol to give 2-(3-aminopropylmercapto)pyridine dihydrobromide (3.2 g.) m.p. 186°-188°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04027026 |
| Source dataset | uspto-grants-1977_05 |
| ORD ID | ord-2204f4dc12e14fd3bed8a3cd38fa7832 |
| Source note | uspto-grants-1977_05 |