HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl Isocyanate → HCID 13498706, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl Isocyanate | HCID 12228 | — |
| Reactant | 2-((2-Aminoethyl)thiomethyl)pyridine | HCID 12889401 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 13498706 | HCID 13498706 | — |
Reaction Steps
A mixture of 2-[(2-aminoethyl)thiomethyl]pyridine (7.0 g.) and methyl isocyanate (2.7 g.) in acetonitrile was heated for 18 hours in a pressure vessel at 100°. After cooling, the solid obtained was collected and recrystallised from acetonitrile/ether to give N-methyl-N'-[2-(2-pyridylmethylthio)ethyl]urea m.p. 63°-66°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04027026 |
| Source dataset | uspto-grants-1977_05 |
| ORD ID | ord-b26e5ea485314a2c933f0e9b11792995 |
| Source note | uspto-grants-1977_05 |