HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triphenyl(propyl)phosphonium iodide → 4-Fluoro-3'-(butenyl)-2'-methyl-benzophenone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triphenyl(propyl)phosphonium iodide | HCID 10982905 | — |
| Reactant | 2-Methyl-3-(p-fluorobenzoyl)-benzaldehyde | HCID 21432895 | — |
| Product | 4-Fluoro-3'-(butenyl)-2'-methyl-benzophenone | HCID 53801019 | — |
Reaction Steps
Using the procedure of Examples 1 and 2, 2-methyl-3-(p-fluorobenzoyl)-benzaldehyde and n-propyl-triphenyl phosphonium iodide were reacted to obtain 4-fluoro-3'-(butenyl)-2'-methyl-benzophenone which was hydrogenated to form 4-fluoro-3'-(n-butyl)-2'-methyl-benzophenone in the form of an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04027040 |
| Source dataset | uspto-grants-1977_05 |
| ORD ID | ord-00bfbadc6bf24c76b22708903d711d72 |
| Source note | uspto-grants-1977_05 |