HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 9250987, compound → HCID 16080835, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 9250987 | HCID 9250987 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 16080835 | HCID 16080835 | — |
Reaction Steps
Methyl 2-(2-nitrophenoxy)benzoate (540 mg, 0.00198 mol) was dissolved in ethyl acetate (20 mL) and palladium on carbon catalyst (270 mg) was added. The mixture was hydrogenated at 57 psi for 2 h. The catalyst was filtered and the solvents were evaporated to yield the title compound. 1H NMR (250 MHz, CDCl3) δ7.83 (dd, 1H), 7.41 (m, 1H), 7.10 (m, 1H), 6.97 (m, 2H), 6.82 (m, 2H), 6.69 (m, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05447957 |
| Source dataset | uspto-grants-1995_09 |
| ORD ID | ord-3aaeb6604fbb4331ac8a03762779fca0 |
| Source note | uspto-grants-1995_09 |