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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2399278Generated: November 2, 2026

HCID 9250987, compound → HCID 16080835, compound

https://huagongshe.com/reaction/2399278

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 9250987HCID 9250987—
CatalystPalladiumHCID 23938—
SolventEthyl AcetateHCID 8857—
ProductHCID 16080835HCID 16080835—

Reaction Steps

Methyl 2-(2-nitrophenoxy)benzoate (540 mg, 0.00198 mol) was dissolved in ethyl acetate (20 mL) and palladium on carbon catalyst (270 mg) was added. The mixture was hydrogenated at 57 psi for 2 h. The catalyst was filtered and the solvents were evaporated to yield the title compound. 1H NMR (250 MHz, CDCl3) δ7.83 (dd, 1H), 7.41 (m, 1H), 7.10 (m, 1H), 6.97 (m, 2H), 6.82 (m, 2H), 6.69 (m, 1H).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05447957
Source datasetuspto-grants-1995_09
ORD IDord-3aaeb6604fbb4331ac8a03762779fca0
Source noteuspto-grants-1995_09