HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-bromobutanimide → Methyl 2-(4-bromomethylphenoxy)-2-(2-chlorophenyl)acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-bromobutanimide | HCID 67184 | — |
| Reactant | Methyl 2-(2-chlorophenyl)-2-(4-methylphenoxy)acetate | HCID 19385716 | — |
| Product | Methyl 2-(4-bromomethylphenoxy)-2-(2-chlorophenyl)acetate | HCID 19385740 | 76.2% |
Reaction Steps
The product of Step B (0.200 g, 0.69 mmol) was brominated with NBS (117 mg, 0.66 mmol) and purified using the procedure described in Step C of Example 3, and afforded 0.186 g (73%) of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05449682 |
| Source dataset | uspto-grants-1995_09 |
| ORD ID | ord-4b3981749b9041e2ac3994ef7de350c5 |
| Source note | uspto-grants-1995_09 |