1-Bromododecane → HCID 67807514, compound

HRID 2399657Notes

Reaction equation

HRID 2399657 reaction equation
CN(C)CCC[C:6]1[CH:14]=[C:13]([N:15]([CH3:17])[CH3:16])[CH:12]=[CH:11][C:7]=1[C:8]([NH2:10])=[O:9].[CH2:19]([Br:31])[CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH3:30]>CC(CC)=O>[Br-:31].[CH2:19]([N+:15]([CH2:13][CH2:12][CH2:11][NH:10][C:8](=[O:9])[C:7]1[CH:6]=[CH:14][C:13]([N:15]([CH3:16])[CH3:17])=[CH:12][CH:11]=1)([CH3:17])[CH3:16])[CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH3:30]

Participants

4

Reactant 2

HCID 89191-BromododecaneHCID 131719123HCID 131719123, compound

Product 1

HCID 67807514HCID 67807514, compound

Reagents, catalysts & solvents 1

HCID 6569Methyl Ethyl KetoneSolvent

Conditions

Temperature
70 °C

Procedure

13.2 g of N- (3-dimethylaminopropyl-p-dimethylaminobenzamide (0.05 mole) from Example 1 and 12.5 g of dodecylbromide (0.05 mole) were dissolved in 30 ml of methylethylketone and maintained at 70° C. for 8 hours. After cooling to ambient temperature the crystalline product (24 g, 93.5% of theoretical) was filtered and recovered.

Workup

  1. temperatureAfter cooling to ambient temperature the crystalline product (24 g, 93.5% of theoretical)
  2. filtrationwas filtered
  3. customrecovered

Sources & evidence

ORD record
ord-4e71359090c04fff8e823f3288c1d7db
Source dataset
uspto-grants-1995_09
Patent number
US05451394

Reaction notes

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