Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 1-Bromododecane | HCID 8919 | — |
| Reactant | HCID 131719123 | HCID 131719123 | — |
| Solvent | Methyl Ethyl Ketone | HCID 6569 | — |
| Product | HCID 67807514 | HCID 67807514 | — |
Reaction Steps
13.2 g of N- (3-dimethylaminopropyl-p-dimethylaminobenzamide (0.05 mole) from Example 1 and 12.5 g of dodecylbromide (0.05 mole) were dissolved in 30 ml of methylethylketone and maintained at 70° C. for 8 hours. After cooling to ambient temperature the crystalline product (24 g, 93.5% of theoretical) was filtered and recovered.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05451394 |
|---|
| Source dataset | uspto-grants-1995_09 |
|---|
| ORD ID | ord-4e71359090c04fff8e823f3288c1d7db |
|---|
| Source note | uspto-grants-1995_09 |
|---|
