HRID2399658

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID18815

Octadecyl chloride

C18H37Cl

HCID3978888

未命名化合物

PRODUCTS

生成物

结构：CCCCCCCCCCCCCCCCCC[N+](C)(C)CCCNC(=O)c1ccc(N(C)C)cc1.[Cl-]

HCID67735953

未命名化合物

PROCEDURE

实验过程

25.6 g of N-(3-dimethylaminopropyl)-p-dimethylaminobenzamide (0.103 mole) from Example 1 and 28.6 g of stearylchloride (0.099 mole) were melted together and kept at 130° C. for 3 hours. Product was crystallized from 250 ml of methylethylketone. Yield was 42 g (77% of theoretical yield).

WORKUP

后处理

customProduct was crystallized from 250 ml of methylethylketone
customYield was 42 g (77% of theoretical yield)

来源与证据

来源类型: Open Reaction Database
ORD 记录: ord-c2948ff93b0a4e79828553c13ad7a958
来源数据集: uspto-grants-1995_09
DOI: 10.6084/m9.figshare.5104873.v1
专利: US05451394
来源说明: uspto-grants-1995_09

反应 SMILES

[CH3:1][N:2]([CH3:18])[CH2:3][CH2:4][CH2:5][NH:6][C:7](=[O:17])[C:8]1[CH:13]=[CH:12][C:11]([N:14]([CH3:16])[CH3:15])=[CH:10][CH:9]=1.[CH2:19]([Cl:37])[CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH2:30][CH2:31][CH2:32][CH2:33][CH2:34][CH2:35][CH3:36]>>[Cl-:37].[CH2:19]([N+:2]([CH2:3][CH2:4][CH2:5][NH:6][C:7](=[O:17])[C:8]1[CH:13]=[CH:12][C:11]([N:14]([CH3:16])[CH3:15])=[CH:10][CH:9]=1)([CH3:18])[CH3:1])[CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH2:30][CH2:31][CH2:32][CH2:33][CH2:34][CH2:35][CH3:36]