HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Chlorooctadecane → Stearyl-[3-(p-Dimethylaminobenzamido)propyl]-Dimethylammonium Chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Chlorooctadecane | HCID 18815 | — |
| Reactant | 4-(dimethylamino)-N-[3-(dimethylamino)propyl]benzamide | HCID 3978888 | — |
| Product | Stearyl-[3-(p-Dimethylaminobenzamido)propyl]-Dimethylammonium Chloride | HCID 67735953 | — |
Reaction Steps
25.6 g of N-(3-dimethylaminopropyl)-p-dimethylaminobenzamide (0.103 mole) from Example 1 and 28.6 g of stearylchloride (0.099 mole) were melted together and kept at 130° C. for 3 hours. Product was crystallized from 250 ml of methylethylketone. Yield was 42 g (77% of theoretical yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05451394 |
| Source dataset | uspto-grants-1995_09 |
| ORD ID | ord-c2948ff93b0a4e79828553c13ad7a958 |
| Source note | uspto-grants-1995_09 |