HuagongsheHuagongshe Chemistry Print Report · For research reference only
Myristyl chloride → Tetradecyl-[3-(p-Dimethylaminobenzamido)propyl]-Dimethylammonium Chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Myristyl chloride | HCID 17043 | — |
| Reactant | 4-(dimethylamino)-N-[3-(dimethylamino)propyl]benzamide | HCID 3978888 | — |
| Product | Tetradecyl-[3-(p-Dimethylaminobenzamido)propyl]-Dimethylammonium Chloride | HCID 15825621 | — |
Reaction Steps
50 g of N-(3-dimethylaminopropyl)-p-dimethylaminobenzamide (0.201 mole) from Example 1 and 47 g of tetradecylchloride (0.195 mole) were melted together and kept at 130° C. for 4 hours. Product was crystallized from 250 ml of ethylacetate; the crystals were washed with another 150 ml of ethylacetate. Yield was 71 g (74% of theoretical yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05451394 |
| Source dataset | uspto-grants-1995_09 |
| ORD ID | ord-caf60ebe87a6448e9d4e4e1649dbf069 |
| Source note | uspto-grants-1995_09 |