Hydrochloric Acid → HCID 19384416, compound

Participants

Reaction Steps

To a solution of 1-triphenylmethylamino-(4-[benzoxazol-2-yl]benzyloxymethyl)cyclopentane (1.24 g; 2.20 mmol) of 1-triphenylmethylamino-(4-[benzoxazol -2-yl]benzyloxymethyl)cyclopentane in ethanol/CH2Cl2 is added ethanolic HCl until ph≅2. This is then stirred for 72 hrs., concentrated to about one-half the volume and the white precipitate which forms is filtered to obtain 1-amino-[4-(benzoxazol-2-yl)benzyloxymethyl]cyclopentane hydrochloride (m.p. >250° C.).

Provenance & Evidence