HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Bromooctane → HCID 67784940, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Bromooctane | HCID 8140 | — |
| Reactant | HCID 54447109 | HCID 54447109 | — |
| Product | HCID 67784940 | HCID 67784940 | 103.2% |
Reaction Steps
Using the procedure of Example 9, 4.8 g of the ethyl ester from Example 6 was alkylated with 4.38 g of 1-bromooctane to provide 5,6,7,8-tetrahydro-6,6-dimethyl-9-octyl-9H-dibenzo[b,d]pyrrole-3-carboxylic acid ethyl ester (7.0 g;100%) as a yellow oil after purification on a small pad of silica gel.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05451600 |
| Source dataset | uspto-grants-1995_09 |
| ORD ID | ord-4e30327fb8874565b427f1270fcef857 |
| Source note | uspto-grants-1995_09 |