1-Bromooctane → HCID 19384542, compound

Participants

Reaction Steps

Using the procedure of Example 9, the alkylation of 7.7 g of 1,2,3,4-tetrahydro-1,1-dimethyl-6-phenylmethoxy-9H-dibenzo[b,d]pyrrole from Example 58 was reacted with 5.48 g of 1-bromooctane to produce 5.3 g (50.5%) of 1,2,3,4-tetrahydro-1,1-dimethyl-6-phenylmethoxy-9-octyl-9H-dibenzo-[b,d]pyrrole as an orange oil after chromatographic purification.

Provenance & Evidence