1-Bromooctane → HCID 19384458, compound

Participants

Reaction Steps

Using the procedure of Example 9, the alkylation of 4.3 g of 1,2,3,4-tetrahydro-3,3-dimethyl-6-phenylmethoxy-9H-dibenzo[b,d]pyrrole from Example 59 was reacted with 2.92 g of 1-bromooctane to produce 5.5 g (94%) of 1,2,3,4-tetrahydro-3,3-dimethyl-6-phenylmethoxy -9-octyl-9H-dibenzo[b,d]pyrrole as a white solid after chromatographic purification.

Provenance & Evidence