HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Bromooctane → HCID 19384471, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Bromooctane | HCID 8140 | — |
| Reactant | HCID 19384493 | HCID 19384493 | — |
| Product | HCID 19384471 | HCID 19384471 | 61.7% |
Reaction Steps
Using the procedure of Example 9, 2.9 g of 1,2,3,4-tetrahydro-1-octyl-6-phenylmethoxy-9H-dibenzo[b,d]pyrrole from Example 62 was alkylated with 1.68 g of 1-bromooctane to produce 2.3 g (61.7%) of rac-1,2,3,4-tetrahydro-1,9-dioctyl-6-phenylmethoxy-9H-dibenzo[b,d]pyrrole as a yellow oil after chromatographic purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05451600 |
| Source dataset | uspto-grants-1995_09 |
| ORD ID | ord-5943a61b091f4364bd8f63f89c5ca3b7 |
| Source note | uspto-grants-1995_09 |