Tetrahydrofuran → HCID 19384529, compound

Participants

Reaction Steps

The hydrogenation of 2.8 g of 1,2,3,4-tetrahydro-6-phenylmethoxy -9-[(4-fluorophenyl)methyl]-9H-dibenzo[b,d]pyrrole from Example 77 was carried out by using the procedure described in Example 86 except that 1:1 tetrahydrofuran-absolute ethyl alcohol was used instead of 1:1 ethyl acetate-absolute ethyl alcohol mixture as a solvent. The crude 5,6,7,8-tetrahydro-9-[(3-fluorophenyl)methyl]-9H-dibenzo[b,d]pyrrol-3-ol was used without further purification.

Provenance & Evidence