HRID2399814

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID5192

Decanedioic acid

C10H18O4

HCID2723671

Tetrabutylammonium Hydroxide

C16H37NO

PRODUCTS

生成物

结构：CCCC[N+](CCCC)(CCCC)CCCC.CCCC[N+](CCCC)(CCCC)CCCC.O=C([O-])CCCCCCCCC(=O)[O-]

HCID21903074

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID887

Methanol

CH4O

PROCEDURE

实验过程

The procedure used was the same as described above by titration of sebacic acid (0.814 g, 4.02×10-3 mol) with 1M tetrabutylammonium hydroxide solution in methanol. After removal of solvent, a quantitative yield (2.75 g) of salt was obtained. FIG. 45 shows a 1H NMR spectrum and FIG. 46 shows a 13C NMR spectrum of the salt in CDCl3.

WORKUP

后处理

customAfter removal of solvent

来源与证据

来源类型: Open Reaction Database
ORD 记录: ord-f3f4880f41e944d9b4a602d9fff1aa42
来源数据集: uspto-grants-1995_09
DOI: 10.6084/m9.figshare.5104873.v1
专利: US05451643
来源说明: uspto-grants-1995_09

反应 SMILES

[C:1]([OH:14])(=[O:13])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][C:10]([OH:12])=[O:11].[OH-].[CH2:16]([N+:20]([CH2:29][CH2:30][CH2:31][CH3:32])([CH2:25][CH2:26][CH2:27][CH3:28])[CH2:21][CH2:22][CH2:23][CH3:24])[CH2:17][CH2:18][CH3:19]>CO>[C:1]([O-:14])(=[O:13])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][C:10]([O-:12])=[O:11].[CH2:29]([N+:20]([CH2:16][CH2:17][CH2:18][CH3:19])([CH2:21][CH2:22][CH2:23][CH3:24])[CH2:25][CH2:26][CH2:27][CH3:28])[CH2:30][CH2:31][CH3:32].[CH2:29]([N+:20]([CH2:16][CH2:17][CH2:18][CH3:19])([CH2:21][CH2:22][CH2:23][CH3:24])[CH2:25][CH2:26][CH2:27][CH3:28])[CH2:30][CH2:31][CH3:32]