Ethenesulfonyl chloride, 2-phenyl- → HCID 53785241, compound

Participants

Reaction Steps

In a manner analogous to that of Example 5, the title compound was prepared from the Boc amine from Example 4 and β-styrenesulfonyl chloride: 1H NMR (400 MHz, CDCl3) δ7.47 (d, 1H, J =15.4 Hz), 7.42-7.33 (m, 5H), 7.11 (s, 4H), 6.77 (d, 1H, J=15.4 Hz), 6.56 (br s, 1H), 4.48 (br s, 1H), 4.10 (br m, 2H), 2.72 (t, 2H, J=7.1 Hz), 1.39 (s, 9H).

Provenance & Evidence