Tert-butyl 4-aminophenethylcarbamate → HCID 19385028, compound

Participants

Reaction Steps

In a manner analogous to that of Example 5, the title compound was prepared from the Boc amine from Example 4 and 5-(pyridin-2-yl)-2-thiophenesulfonyl chloride: 1H NMR (400 MHz, CD3OD) 8.48 (d, 1, H, J=5.2 Hz), 7.81 (m, 2H), 7.54 (d, 1H, J=4.1 Hz), 7.41 (m, 1H), 7.30 (m, 1H), 7.11 (s, 4H), 3.18 (t, 2H, J=7.1 Hz), 2.67 (t, 2H, J=7.1 Hz), 1.38 (s, 9H). FAB MS m/z 460 (M+1).

Provenance & Evidence