HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylamine → HCID 14578461, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | HCID 19382148 | HCID 19382148 | — |
| Product | HCID 14578461 | HCID 14578461 | — |
Reaction Steps
9.3 g (54.3 mmol) of methyl 5-aza-1-oxaspiro[2,5]octane-5-carboxylate are added dropwise to 50 ml of methylamine solution (25% in water) and the mixture is stirred overnight at room temperature. It is then concentrated and the residue is distilled.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05453422 |
| Source dataset | uspto-grants-1995_09 |
| ORD ID | ord-37e0c194a5d3413dab5222676e0da90e |
| Source note | uspto-grants-1995_09 |