HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylamine → HCID 19382193, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | Ethyl 1-oxa-6-azaspiro[2,5]octane-6-carboxylate | HCID 13672926 | — |
| Product | HCID 19382193 | HCID 19382193 | — |
Reaction Steps
5.2 g (28 mmol) of ethyl 6-aza-1-oxaspiro[2,5]-octane-6-carboxylate are added dropwise to 30 ml of methylamine solution (25% in water) and the mixture is stirred overnight at room temperature. It is then concentrated and recrystallized from petroleum ether (hygroscopic crystals).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05453422 |
| Source dataset | uspto-grants-1995_09 |
| ORD ID | ord-fac9ac652b8749cf9bf84992d7ccf1be |
| Source note | uspto-grants-1995_09 |