HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 178499517, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | HCID 178433551 | HCID 178433551 | — |
| Product | HCID 178499517 | HCID 178499517 | 79% |
Reaction Steps
A solution of (4-hydroxy-2-mercapto-6-methyl-5-pyrimidinyl)-acetic acid (190 g, 0.95 mol) and concentrated sulfuric acid (50 ml) in methanol (1.51) is refluxed for 18 hours. The suspension is cooled and filtered to give methyl(4-hydroxy-2-mercapto-6-methyl-5-pyrimidinyl)-acetate (160 g, 79%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05453427 |
| Source dataset | uspto-grants-1995_09 |
| ORD ID | ord-b0304f52e178408b8d523fa1c817dbbe |
| Source note | uspto-grants-1995_09 |