HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tetrahydrofuran → HCID 10130365, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tetrahydrofuran | HCID 8028 | — |
| Reactant | 1H-Indazole | HCID 9221 | — |
| Reactant | Chloroformamidinium chloride | HCID 3084509 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 10130365 | HCID 10130365 | 52.8% |
Reaction Steps
940 mg of indazole and 920 mg of chloroformamidine hydrochloride were heated under reflux in 30 ml of benzene of THF for 5 hours, and the crystals formed were removed by filtration. These were recrystallized from ethanol ether to obtain 826 mg of 2H-indazole-2-carboxamidine hydrochloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05453514 |
| Source dataset | uspto-grants-1995_09 |
| ORD ID | ord-f5e371b5f6f84d5fa3d0c063e1752870 |
| Source note | uspto-grants-1995_09 |