HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2400314Generated: November 1, 2026
Triphenylphosphine → HCID 86629717, compound
https://huagongshe.com/reaction/2400314
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Triphenylphosphine | HCID 11776 | — |
| Reactant | HCID 57661602 | HCID 57661602 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 86629717 | HCID 86629717 | — |
Reaction Steps
To 5-bromomethylthiophene-2-carboxylic acid tert-butyl ester (14.9 mmol, 43.8 mmol) was added toluene (300 mL) and triphenylphosphine (14.1 g, 53.8 mmol). The mixture was heated to 70° C. overnight. The solvent was remove in vacuo to give (5-tert-Butoxycarbonyl-thiophen-2-ylmethyl)-triphenylphosphonium bromide
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08796205B2 |
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| Source dataset | uspto-grants-2014_08 |
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| ORD ID | ord-1e0cb72583014a2597378bafe757e9c8 |
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| Source note | uspto-grants-2014_08 |
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