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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2400361Generated: November 3, 2026

Diethyl Ether → HCID 67029295, compound

https://huagongshe.com/reaction/2400361

Reaction equation

Participants

RoleNameHCIDCharge
ReactantDiethyl EtherHCID 3283—
ReactantN-IodosuccinamideHCID 21864724—
ReactantHCID 67027581HCID 67027581—
SolventDimethylformamideHCID 6228—
ProductHCID 67029295HCID 6702929539.6%

Reaction Steps

7-(5-Methyl-[1,2,4]triazin-3-yl)-imidazo[1,2-a]pyridine (200 mg, 0.9 mmol, 1 equiv) and N-iodosuccinamide (300 mg, 1.3 mmol, 1.4 equiv) in dimethylformamide (5 ml) was stirred at room temperature. After 3 hours diethyl ether was added and the resultant solid was isolated by vacuum filtration furnishing 120 mg of a yellow solid. MS: [M+H]+338

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08796244B2
Source datasetuspto-grants-2014_08
ORD IDord-8cd74c3a345f45f098a385d061f6cc11
Source noteuspto-grants-2014_08