HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl Ether → HCID 67029295, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | N-Iodosuccinamide | HCID 21864724 | — |
| Reactant | HCID 67027581 | HCID 67027581 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 67029295 | HCID 67029295 | 39.6% |
Reaction Steps
7-(5-Methyl-[1,2,4]triazin-3-yl)-imidazo[1,2-a]pyridine (200 mg, 0.9 mmol, 1 equiv) and N-iodosuccinamide (300 mg, 1.3 mmol, 1.4 equiv) in dimethylformamide (5 ml) was stirred at room temperature. After 3 hours diethyl ether was added and the resultant solid was isolated by vacuum filtration furnishing 120 mg of a yellow solid. MS: [M+H]+338
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08796244B2 |
| Source dataset | uspto-grants-2014_08 |
| ORD ID | ord-8cd74c3a345f45f098a385d061f6cc11 |
| Source note | uspto-grants-2014_08 |