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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2400753Generated: November 1, 2026

HCID 131731727, compound → HCID 90228699, compound

https://huagongshe.com/reaction/2400753

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 131731727HCID 131731727—
CatalystPalladiumHCID 23938—
SolventMethanolHCID 887—
ProductHCID 90228699HCID 9022869983%

Reaction Steps

To a solution of compound 286 (0.22 g, 0.44 mmol) in 10 mL of CH3OH was added 0.1 g of Pd—C (10%, wet). The mixture was hydrogenated at room temperature for 16 h. The catalyst was removed by filtration through a pad of celite. The filtrate was concentrated to afford compound 287 as a solid (0.15 g, 83%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08796257B2
Source datasetuspto-grants-2014_08
ORD IDord-99da7805437d40f687a8703b223d5950
Source noteuspto-grants-2014_08