HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(4-chloro-2-(trifluoromethyl)benzyl)-1H-indazole-5-carbaldehyde → HCID 58530960, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(4-chloro-2-(trifluoromethyl)benzyl)-1H-indazole-5-carbaldehyde | HCID 86654547 | — |
| Reactant | HCID 86659693 | HCID 86659693 | — |
| Product | HCID 58530960 | HCID 58530960 | — |
| Product | HCID 86659692 | HCID 86659692 | — |
Reaction Steps
(5Z)-{5-[1-(4-Chloro-2-trifluoromethylbenzyl)-1H-indazol-5-ylmethylene]-2,4-dioxothiazolidin-3-yl}carbamic acid tert-butyl ester was prepared from (2,4-dioxothiazolidin-3-yl)carbamic acid tert-butyl ester and [4-chloro-2-(trifluoromethyl)benzyl]-1H-indazol-5-carbaldehyde (from Example 1) following General Procedure F1. The Boc group was removed by TFA/DCM following General Procedure M to afford the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08796256B2 |
| Source dataset | uspto-grants-2014_08 |
| ORD ID | ord-fe78890b00884b55820210f700bd7d3a |
| Source note | uspto-grants-2014_08 |