HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 519849, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Phthalic Anhydride | HCID 6811 | — |
| Reactant | 4-Methoxybenzylamine | HCID 75452 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 519849 | HCID 519849 | — |
Reaction Steps
4-Methoxybenzylamine (4.9 g, 36 mmol) was added to phthalic anhydride (4.5 g, 30 mmol) in 15 mL glacial acetic acid. The reaction was stirred at 100° C. for 4 h as water was collected with a Dean-Stark trap. Solvent was evaporated and the product was obtained by crystallization from ethanol (7 g, 87%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08796313B2 |
| Source dataset | uspto-grants-2014_08 |
| ORD ID | ord-fbb5cd5062ed4b99b9f884e2a485fcc2 |
| Source note | uspto-grants-2014_08 |