Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Aspirin | HCID 2244 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | Didecyldimethylammonium Chloride | HCID 23558 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 69295493 | HCID 69295493 | 90% |
Reaction Steps
A stoichiometric mixture of didecyldimethylammonium chloride, acetylsalicyclic acid, and NaOH in distilled water was stirred at 60° C. for 2 h and then cooled to room temperature. The aqueous solution was extracted by chloroform. Chloroform was removed and prepared didecyldimethylammonium 2-acetoxybenzoate with 90% yield was dried in vacuum.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08802596B2 |
|---|
| Source dataset | uspto-grants-2014_08 |
|---|
| ORD ID | ord-934c959fd339492883d9988528f3b951 |
|---|
| Source note | uspto-grants-2014_08 |
|---|
